Research Check-In Part 3

It has been confirmed by spectroscopy techniques that my desired ligand has been synthesized, although in small quantity. The next step is to attach the ligand to a metal in order to form a catalytic compound. The chemical reaction which combines the ligand and the metal was performed and the resulting substance was allowed to sit undisturbed in an attempt to crystallize. In the method of crystallization I am using, the substance is dissolved in a liquid solvent #1, which is placed either below or on top of a liquid solvent #2 in a vial. The substance cannot be dissolved in solvent #2. As solvents #1 and #2 begin to mix, the substance slowly travels from #1 to #2 and precipitates out into solid crystals. Once the crystals have precipitated, they can be electrochemically tested for hydrogen oxidation.

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